Expanding the synthesis of Stober spheres: towards the synthesis of nano-magnesium oxide and nano-zinc oxide
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Publication Details
Author list: Mguni LL, Mukenga M, Muzenda E, Jalama K, Meijboom R
Publisher: Springer
Place: DORDRECHT
Publication year: 2013
Journal: Journal of Sol-Gel Science and Technology (0928-0707)
Journal acronym: J SOL-GEL SCI TECHN
Volume number: 66
Issue number: 1
Start page: 91
End page: 99
Number of pages: 9
ISSN: 0928-0707
eISSN: 1573-4846
Languages: English-Great Britain (EN-GB)
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Abstract
In order to synthesise Stober spheres of different diameters, fixed amounts of ethanol, ammonia and water were used with varying amounts of tetraethyl orthosilicate. This simple method was further applied to the synthesis of nano-ZnO and nano-MgO from their respective precursors, zinc methoxide and magnesium ethoxide. The spherical nano-SiO2, nano-ZnO and nano-MgO synthesised in this way were characterised by X-ray diffraction, Fourier-transform infrared spectroscopy, scanning electron microscopy and transmission electron microscopy. Preliminary investigations found that nano-ZnO and nano-MgO showed good catalytic activity in the trans-esterification reaction that converts vegetable oil to biodiesel.
Keywords
Nano-MgO, Nano-ZnO, Precursors, Silica, Stober method, Trans-esterification
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